مهندسی شیمی ایران

مهندسی شیمی ایران

شبیه‌سازی شرایط عملیاتی استخراج سبز ساپونین از چوبک تحت شرایط آب مادون بحرانی و بررسی خواص آن

نوع مقاله : مقاله پژوهشی

نویسندگان
1 دانشجوی دکتری مهندسی شیمی، دانشگاه صنعتی سهند
2 دانشیار مهندسی شیمی، دانشگاه صنعتی سهند
3 استادیار مهندسی شیمی، دانشگاه کردستان
چکیده
استفادهاز آب در شرایط مادون بحرانی (دما و فشار بالای 100 درجۀ سلسیوس و 1 اتمسفر) باعث تغییر قطبیت آن بهسمت حلالهای آلی می‌شود که به‌راحتی می‌توان از آن در استخراج ترکیبات باارزش از منابع گیاهی استفاده کرد. در پژوهش حاضر، شبیه‌سازی شرایط عملیاتی استخراج ساپونین از چوبک بهروش آب مادون بحرانی بااستفادهاز نرم‌افزار شبیه‌ساز  انجام پذیرفت. نتایج شبیه‌سازی نشان داد که با اعمال دمای خارجی 120، 140، 160، 180 و 200 درجۀ سلسیوس بعد از زمان 120 دقیقه، دمای آب مادون بحرانی داخل اتوکلاو بهترتیب 107، 124، 144، 161 و 178 درجۀ سلسیوس است. استخراج ساپونین با دو روش خیساندن در آب و آب مادون بحرانی انجام شد؛ نتایج نشان داد که میزان چربی موجود در چوبک 3% وزنی است. نتایج داده‌های شبیه‌سازی نشان داد که در شرایط دمایی 130 درجۀ سلسیوس و زمان 120 دقیقه، دمای آب درون اتوکلاو 116 درجۀ سلسیوس است. هم‌چنین، نتایج استخراج نشان داد که میزان کفکنندگی و قدرت امولسیونکنندگی در نمونۀ استخراجی با آب مادون بحرانی بهترتیب 2/7 و 1/5 برابر نمونۀ استخراجی با آب است.
کلیدواژه‌ها

موضوعات


عنوان مقاله English

Simulation of the Operation Conditions for Saponin Green Extraction from Chubak Using Subcritical Water and Evaluation of Their Characteristics

نویسندگان English

Sh. Nasiri 1
H. Jafarizadeh 2
O. Ahmadi 3
1 Ph. D. Student of Chemical Engineering, Sahand University of Technology
2 Associate Professor of Chemical Engineering, Sahand University of Technology
3 Assistant Professor of Chemical Engineering, University of Kurdistan
چکیده English

Using subcritical water (temperature and pressure of higher than 100 ºC and 1 atm) polarity of water changes into the organic solvents which that can be easily used in extraction of the valuable components from the plant sources. In the present study, simulation of the operation conditions for saponin extraction from the Chubak and using subcritical water was accomplished. Results indicated that by placing the of autoclove in the oven adjusted at temperatures of 120, 140, 160, 180 and 200 ºC, after 120 min the international temperastures of the water inside the autoclove were 107, 124, 144, 161 and 178 ºC, respectively. Saponin extraction was done using water at 130 ºC and 120 min and the result indicated that the water inside of autoclove had temperature of 116 ºC, which that was in subcritical state. The result revealed that lipid content of Chubak was 3% (W/W). Furthermore, extraction results indicated that the foaming height and emulsification capacity of the extracted sample using subcritical water were 2.7 and 1.5 folds higher than those of the extracted sample using water.

کلیدواژه‌ها English

Chubak
Green Extraction
Saponin
Simulation
Subcritical Water
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