مطالعۀ آزمایشگاهی استخراج عطرمایۀ‌ روغنی از گیاه کک‌گریز با استفاده از دی‌اکسید کربن فوق بحرانی

نوع مقاله : مقاله پژوهشی

نویسندگان

گروه مهندسی شیمی، واحد مرودشت، دانشگاه آزاد اسلامی، مرودشت، ایران

چکیده

روش استخراج به‌‌کمک دی‌اکسید کربن فوق بحرانی بهدلیل دمای کم عملیات و نبودن حلال در محصول نهایی، جایگزین روشهای قدیمی استخراج شدهاست. در این تحقیق تأثیر تغییر سه مؤلفۀ دما (35، 45، 55 درجۀ سلسیوس)، فشار (150،175، 200 بار) و اندازۀ ذره (074/0،149/0، 210/0 میلیمتر) بر بازده عطرمایۀ روغنی استخراجشده از گیاه دارویی ککگریز با دیاکسید کربن فوق بحرانی مطالعه شد. نتایج حاصل از آزمایشها نشانداد که میزان استخراج با کاهش اندازۀ ذرات و افزایش فشار، افزایش یافت. افزایش دما تا 45 درجۀ سلسیوس تأثیر مثبتی در بازده استخراج دارد؛ اما با افزایش دما بیشتر از
45 درجۀ سلسیوس، کاهش بازدهی مشاهده شد. در شرایط فشار 200 بار و دمای
45 درجۀ سلسیوس و اندازۀ ذرۀ 074/0 میلی‌متر، بیشترین میزان استخراج
حاصل شده
است.

کلیدواژه‌ها


عنوان مقاله [English]

Experimental Study Extraction Oil from Francoeuria Undulata Using Supercritical Carbon Dioxide

نویسندگان [English]

  • M. Kasraei
  • N. Esfandiari
  • B. Honarvar
Marvdasht Branch, Islamic Azad University
چکیده [English]

Supercritical fluid extraction method is a replacement of conventional methods such as organic solvent extraction with hexane and mechanical pressing. Because in this method the operation temperature is low and the solvent does not remain in the final product. In this study, the effect of changing three parameters of temperature (35, 45, 55 °C), pressure (150, 175, 200 bar) and particle size (0.074, 0.149, 0.210 mm) on the extracted oil yield of the medicinal plant of Francoeuria undula using supercritical carbon dioxide was investigated. The results of the experiments showed that the extraction yield was increased by particle size reduction and increased pressure. Temperature up to 45 ºC has a positive impact on the extraction efficiency. However, increased efficiency was observed with increasing temperature more than of 45 °C. The best extraction yield in conditions of pressure was 200 bar, temperature 45 °C and particle size of 0.074 mm.

کلیدواژه‌ها [English]

  • Extraction
  • Essential Oil
  • Supercritical Carbon Dioxide
  • Francoeuria Undula
  • Taguchi Method
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